The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 23, 2020

Filed:

Jul. 30, 2015
Applicant:

National Institute of Advanced Industrial Science and Technology, Tokyo, JP;

Inventors:

Kunimitsu Kataoka, Tsukuba, JP;

Junji Akimoto, Tsukuba, JP;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
H01M 10/0562 (2010.01); H01M 10/0525 (2010.01); C01G 25/00 (2006.01); C30B 13/28 (2006.01); C30B 29/22 (2006.01); C30B 15/20 (2006.01);
U.S. Cl.
CPC ...
H01M 10/0562 (2013.01); C01G 25/00 (2013.01); C01G 25/006 (2013.01); C30B 13/28 (2013.01); C30B 15/20 (2013.01); C30B 29/22 (2013.01); H01M 10/0525 (2013.01); C01P 2002/30 (2013.01); C01P 2002/70 (2013.01); C01P 2002/72 (2013.01); C01P 2002/77 (2013.01); C01P 2004/01 (2013.01); C01P 2006/10 (2013.01); C01P 2006/40 (2013.01); H01M 2220/30 (2013.01); H01M 2300/0071 (2013.01);
Abstract

Provided is a high-density lithium-containing garnet crystal body. The lithium-containing garnet crystal body has a relative density of 99% or more, belongs to a tetragonal system, and has a garnet-related type structure. A method of producing a LiLaZrOcrystal, which is one example of this lithium-containing garnet crystal body, includes melting a portion of a rod-like raw material composed of polycrystalline LiLaZrObelonging to a tetragonal system while rotating it on a plane perpendicular to the longer direction and moving the melted portion in the longer direction. The moving rate of the melted portion is preferably 8 mm/h or more but not more than 19 mm/h. The rotational speed of the raw material is preferably 30 rpm or more but not more than 60 rpm. By increasing the moving rate of the melted portion, decomposition of the raw material due to evaporation of lithium can be prevented and by increasing the rotational speed of the raw material, air bubbles can be removed.


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