The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 02, 2020

Filed:

Jan. 16, 2017
Applicants:

Institute of Process Engineering, Chinese Academy of Sciences, Beijing, CN;

Beijing Zhongkaihongde Technology Co., Ltd, Beijing, CN;

Inventors:

Chuanlin Fan, Beijing, CN;

Qingshan Zhu, Beijing, CN;

Haitao Yang, Beijing, CN;

Wenheng Mu, Beijing, CN;

Jibin Liu, Beijing, CN;

Cunhu Wang, Beijing, CN;

Qixun Ban, Beijing, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01M 8/18 (2006.01); B01J 8/00 (2006.01); B01J 8/18 (2006.01); B01J 8/26 (2006.01); C01G 31/02 (2006.01);
U.S. Cl.
CPC ...
H01M 8/188 (2013.01); B01J 8/0045 (2013.01); B01J 8/0055 (2013.01); B01J 8/1827 (2013.01); B01J 8/1836 (2013.01); B01J 8/26 (2013.01); C01G 31/02 (2013.01); H01M 8/18 (2013.01); B01J 2208/00752 (2013.01); B01J 2208/00761 (2013.01); B01J 2208/00893 (2013.01); C01P 2006/80 (2013.01); H01M 2300/0011 (2013.01); Y02E 60/528 (2013.01);
Abstract

A system and method for producing a 3.5-valence high-purity vanadium electrolyte, comprising hydrolyzing high-purity vanadium oxytrichloride into vanadium pentoxide in a fluidized bed, and reducing vanadium pentoxide into a low-valence vanadium oxide having an average vanadium valence of 3.5 adding water and a sulfuric acid solution under a microwave field applied externally for dissolution at a low temperature, to obtain a 3.5-valence high-purity vanadium electrolyte. The preparation of vanadium pentoxide by means of gas-phase hydrolysis in the fluidized bed is of short process and high efficiency. By providing an internal member within the reduction fluidized bed, the precise regulation of the valence state of the reduction product is achieved, and the special chemical effect of the microwave field is used to promote dissolution of the vanadium oxide and activate the vanadium ions, thereby greatly improving the activity of the electrolyte.


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