The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 12, 2020

Filed:

Dec. 09, 2014
Applicant:

Arkema France, Colombes, FR;

Inventors:

Serge Tretjak, Roulhing, FR;

Anne Moreliere, Longeville-les-St-Avold, FR;

Assignee:

ARKEMA FRANCE, Colombes, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/56 (2006.01); B01D 61/36 (2006.01); C07C 67/08 (2006.01); B01D 71/02 (2006.01); B01D 71/38 (2006.01); B01D 3/14 (2006.01);
U.S. Cl.
CPC ...
C07C 67/56 (2013.01); B01D 3/145 (2013.01); B01D 61/362 (2013.01); B01D 71/028 (2013.01); B01D 71/38 (2013.01); C07C 67/08 (2013.01); B01D 2311/2669 (2013.01); Y02P 20/582 (2015.11);
Abstract

The invention relates to a method for producing alkyl (meth)acrylate comprising a linear or branched alkyl chain comprising 4 to 10 carbon atoms, by direct esterification of (meth)acrylic acid with a linear or branched alcohol comprising 4 to 10 carbon atoms in the presence of a catalyst, leading to formation of a reaction mixture comprising the desired ester, unreacted acid and alcohol, light by-products, and heavy by-products. The mixture undergoes purification treatment by separation means to obtain purified alkyl (meth)acrylate. The purification treatment comprises a step of membrane separation dehydration applied to at least one of the following: the stream subjected to the final distillation leading to the recovery of the purified (meth)acrylic ester, the aqueous stream originating from the settling out of the reaction mixture, or the stream resulting from the distillation of the light by-products present in the reaction mixture.


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