The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 14, 2020

Filed:

Sep. 20, 2017
Applicant:

Nanjing University, Nanjing, CN;

Inventors:

Ke Xu, Nanjing, CN;

Shuhan Wen, Nanjing, CN;

Hongqiang Ren, Nanjing, CN;

Jinju Geng, Nanjing, CN;

Assignee:

NANJING UNIVERSITY, Nanjing, CN;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01J 37/04 (2006.01); B01J 37/08 (2006.01); B01J 37/06 (2006.01); B01J 21/16 (2006.01); B01J 37/34 (2006.01); B01J 21/00 (2006.01); B01J 35/02 (2006.01); B01J 35/08 (2006.01); B01J 23/00 (2006.01); C02F 1/78 (2006.01); C02F 1/72 (2006.01); B01J 23/34 (2006.01);
U.S. Cl.
CPC ...
B01J 37/04 (2013.01); B01J 21/005 (2013.01); B01J 21/16 (2013.01); B01J 23/005 (2013.01); B01J 23/34 (2013.01); B01J 35/023 (2013.01); B01J 35/026 (2013.01); B01J 35/08 (2013.01); B01J 37/06 (2013.01); B01J 37/08 (2013.01); B01J 37/343 (2013.01); B01J 37/346 (2013.01); C02F 1/725 (2013.01); C02F 1/78 (2013.01);
Abstract

A method for preparing a catalyst, including: 1) uniformly mixing attapulgite, lithium-manganese spinel (Li—Mn spinel), manganese dioxide powders to form mixed raw material; adding water to the mixed raw material; stirring and mixing the mixed raw material and the water for between 5 and 15 min to yield a reaction mixture; 2) feeding the reaction mixture in 1) to a pelletizer to prepare spherical particles or hollow cylindrical particles; drying the spherical particles or the hollow cylindrical particles to yield a precursor; 3) heating the precursor in a muffle furnace, and calcining the precursor to yield a crude catalyst; 4) mixing the crude catalyst with an acid solution; alternating between ultrasound and microwave to wash the crude catalyst; and 5) washing the crude catalyst in 4) with water; and drying the catalyst for 12 hrs in air at 105° C.


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