The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 24, 2020

Filed:

Dec. 14, 2016
Applicant:

Fondazione Istituto Italiano Di Tecnologia, Genoa, IT;

Inventors:

Mauro Moglianetti, Civitanova Marche, IT;

Pier Paolo Pompa, Lecce, IT;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B22F 9/24 (2006.01); C30B 7/14 (2006.01); C30B 29/02 (2006.01); C30B 29/60 (2006.01); B22F 1/00 (2006.01); C30B 29/66 (2006.01); B82Y 40/00 (2011.01);
U.S. Cl.
CPC ...
B22F 9/24 (2013.01); B22F 1/0018 (2013.01); C30B 7/14 (2013.01); C30B 29/02 (2013.01); C30B 29/60 (2013.01); C30B 29/66 (2013.01); B22F 2001/0037 (2013.01); B22F 2301/25 (2013.01); B22F 2304/054 (2013.01); B22F 2998/00 (2013.01); B82Y 40/00 (2013.01);
Abstract

The present disclosure relates to a seed-growth based method for the synthesis of metal nanoparticles of controlled shape (cubes, cuboids, octahedrons) and size in an aqueous environment, without the use of shape directing agents. The method involves a first step of preparing a solution comprising water, metal seed growth nanoparticles, a metal salt comprising the same metal as the metal seed growth nanoparticles, and a reducing agent; and a second step of heating the solution to between 9 and 130° C. at a rate of between 1° C./min and 5° C./min and at a pressure of between 1 and 5 atm. The method may also be carried out in a reduced oxygen atmosphere and the concentration of oxygen disclosed in the solution may be less than the concentration of oxygen in an oxygen saturated solution.


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