The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 10, 2020

Filed:

Sep. 13, 2016
Applicants:

Viktor Veniaminovich Tets, St. Petersburg, RU;

Georgy Viktorovich Tets, St. Petersburg, RU;

Inventors:

Viktor Veniaminovich Tets, St. Petersburg, RU;

Georgy Viktorovich Tets, St. Petersburg, RU;

Viktor Iosifovich Krutikov, St. Petersburg, RU;

Assignee:

Other;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 315/04 (2006.01); C07C 311/44 (2006.01); C07C 303/38 (2006.01); C07C 311/21 (2006.01); C07C 317/42 (2006.01);
U.S. Cl.
CPC ...
C07C 315/04 (2013.01); C07C 303/38 (2013.01); C07C 311/21 (2013.01); C07C 311/44 (2013.01); C07C 317/42 (2013.01);
Abstract

The invention relates to the field of organic chemistry and medicine, and more particularly to a method of producing synthetic biologically active derivatives of carbopentoxysulfanilic acid. The present method of producing a sodium salt of (2,6-dichlorophenyl)amide carbopentoxysulfanilic acid is characterized in that the reaction mass formed during the production of (2,6-dichlorophenyl)amide carbopentoxysulfanilic acid is agitated in a medium which is acidified with a solution of hydrochloric acid to pH 5-5.5, and the isolated precipitate may be washed with water acidified with a solution of hydrochloric acid to pH 5-5.5. This increases the yield of a sodium salt of (2,6-dichlorophenyl)amide carbopentoxysulfanilic acid to 70% (compared to a prior art yield of 32%) and also increases the purity of the target sodium salt.


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