The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 25, 2020

Filed:

Nov. 09, 2015
Applicant:

Battelle Memorial Institute, Columbus, OH (US);

Inventors:

Amy M Heintz, Dublin, OH (US);

Chad M. Cucksey, Worthington, OH (US);

Anthony D. Duong, Columbus, OH (US);

Randy L. Jones, Delaware, OH (US);

Michael D. Crenshaw, Orient, OH (US);

Assignee:

Battelle Memorial Institute, Columbus, OH (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C09D 5/24 (2006.01); C09D 7/40 (2018.01); C08J 5/00 (2006.01); C08B 37/08 (2006.01); C01B 32/174 (2017.01); C09D 105/08 (2006.01); C08L 5/08 (2006.01); H01B 1/24 (2006.01);
U.S. Cl.
CPC ...
C09D 5/24 (2013.01); C01B 32/174 (2017.08); C08B 37/0072 (2013.01); C08J 5/005 (2013.01); C08L 5/08 (2013.01); C09D 7/70 (2018.01); C09D 105/08 (2013.01); H01B 1/24 (2013.01); C08J 2305/08 (2013.01); C08J 2305/12 (2013.01);
Abstract

A method of making CNT films is described in which the film is washed with a mild acid treatment. The method generates a CNT film that is not sensitive to moisture or fluctuations in moisture. The method involves the use of anionic polysaccharides or anionic glycosaminoglycans such as hyaluronic acid, sodium salt, as aqueous dispersing agents and their modification to a hydrophobic matrix after deposition. In the course of conducting the work described here, we made the surprising discovery that washing with an aqueous acidic solution resulted in a decrease in resistance through the material. The invention also includes CNT composites made by the inventive methods and a CNT composite comprising CNTs and anionic polysaccharides or anionic glycosaminoglycans further characterized by a low cationic content and a high conductivity and/or small CNT particle size as measured by SEM.


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