The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 18, 2020

Filed:

Jun. 13, 2013
Applicant:

University of Maine System Board of Trustees, Orono, ME (US);

Inventors:

Michael A. Bilodeau, Brewer, ME (US);

Mark A. Paradis, Old Town, ME (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
D21C 9/00 (2006.01); D21H 11/18 (2006.01); D21H 17/00 (2006.01); D21H 17/63 (2006.01);
U.S. Cl.
CPC ...
D21C 9/007 (2013.01); D21C 9/002 (2013.01); D21C 9/004 (2013.01); D21H 11/18 (2013.01); D21H 17/005 (2013.01); D21H 17/63 (2013.01);
Abstract

A scalable, energy efficient process for preparing cellulose nanofibers is disclosed. The process employs a depolymerizing treatment with one or both of: (a) a relatively high charge of ozone under conditions that promote the formation of free radicals to chemically depolymerize the cellulose fiber cell wall and interfiber bonds; or (b) a cellulase enzyme. Depolymerization may be estimated by pulp viscosity changes. The depolymerizing treatment is followed by or concurrent with mechanical comminution of the treated fibers, the comminution being done in any of several mechanical comminuting devices, the amount of energy savings varying depending on the type of comminuting system and the treatment conditions. Comminution may be carried out to any of several endpoint measures such as fiber length, % fines or slurry viscosity.


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