The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 11, 2020

Filed:

Jan. 28, 2016
Applicant:

Novartis Ag, Basel, CH;

Inventors:

Andreas Bertogg, Aarau, CH;

Hanspeter Schilling, Bottmingen/BL, CH;

Assignee:

Novartis AG, Basel, CH;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 487/00 (2006.01); C07D 233/54 (2006.01); A61K 31/4184 (2006.01); C07D 403/10 (2006.01); C07D 487/04 (2006.01); C07D 471/04 (2006.01); C07D 473/00 (2006.01);
U.S. Cl.
CPC ...
C07D 233/54 (2013.01); A61K 31/4184 (2013.01); C07D 403/10 (2013.01); C07D 487/04 (2013.01);
Abstract

The present invention relates to a process for providing the compound of formula I, comprising the step of reacting a compound of formula VII with a base in the presence of an alkaline- or alkaline earth metal salt (MX), wherein LG is a leaving group. The presence of an alkaline- or alkaline earth metal salt was surprisingly found to render said reaction highly reliable in terms of the yield and purity of the compound of formula I obtained. In a further aspect, the present invention relates to the compound of formula I, having less than an amount of 1.50% or less than an amount of 1.25% or less than an amount of 1.00% or less than an amount of 0.75% or less than an amount of 0.50% or less than an amount of 0.25% or less than an amount of 0.10% of the compound of formula VIII.


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