The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 21, 2020

Filed:

Aug. 19, 2016
Applicants:

Beijing Yuji Science & Technology Co., Ltd., Haidian District, Beijing, CN;

Zeon Corporation, Chiyoda-ku, Tokyo, JP;

Inventors:

Hengdao Quan, Beijing, CN;

Dongpeng Liu, Beijing, CN;

Xiaoqing Jia, Beijing, CN;

Xiaomeng Zhou, Beijing, CN;

Assignees:

Beijing Yuji Science & Technology Co., Ltd., Haidian District, CN;

ZEON CORPORATION, Chiyoda-ku, Tokyo, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 17/20 (2006.01); B01J 23/26 (2006.01); B01J 23/28 (2006.01); B01J 23/30 (2006.01); B01J 37/08 (2006.01); C07C 4/22 (2006.01); C07C 17/02 (2006.01);
U.S. Cl.
CPC ...
C07C 17/206 (2013.01); B01J 23/26 (2013.01); B01J 23/28 (2013.01); B01J 23/30 (2013.01); B01J 37/08 (2013.01); C07C 4/22 (2013.01); C07C 17/02 (2013.01);
Abstract

Disclosed is a manufacturing method of 1,2-dichlorohexafluorocyclopentene. The first reaction uses dicyclopentadiene as a starting material and nitrogen gas or another inert gas as a diluting agent in a gas-phase thermal cracking reaction to obtain cyclopentadiene. The second reaction uses cyclopentadiene as a starting material in a liquid phase chlorination reaction with chlorine gas to obtain 1,2,3,4-tetrachlorocyclopentane. The third reaction uses 1,2,3,4-tetrachlorocyclopentane as a starting material in a gas-phase chlorination and fluorination reaction with hydrogen fluoride and chlorine gas in the presence of a chromium-based catalyst to obtain 1,2-dichlorohexafluorocyclopentene. The method uses easily acquired starting material and a stable fluorination catalyst, provides a high yield for a target product, and is applicable for large-scale continuous gas-phase production of 1,2-dichlorohexafluorocyclopentene.


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