The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 31, 2019

Filed:

Nov. 11, 2016
Applicant:

Waters Technologies Corporation, Milford, MA (US);

Inventor:

Michael S. Young, Bellingham, MA (US);

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
G01N 33/64 (2006.01); G01N 30/72 (2006.01); B01D 15/26 (2006.01); G01N 30/88 (2006.01); G01N 1/34 (2006.01); G01N 1/40 (2006.01); G01N 30/00 (2006.01); G01N 30/02 (2006.01);
U.S. Cl.
CPC ...
G01N 33/64 (2013.01); B01D 15/26 (2013.01); G01N 30/7233 (2013.01); G01N 30/88 (2013.01); G01N 1/34 (2013.01); G01N 1/405 (2013.01); G01N 2001/4061 (2013.01); G01N 2030/009 (2013.01); G01N 2030/027 (2013.01); G01N 2430/10 (2013.01); G01N 2560/00 (2013.01);
Abstract

The technology of the present application is directed to methods and kits for detecting and quantifying a non-polar analyte in a plant-derived sample. The technology uses a simple extraction, e.g., a liquid-liquid extraction (LLE) or solid-phase extraction (SPE), to enrich a sample for a non-polar analyte of interest and to remove contaminants. After the extraction and clean-up steps, liquid chromatography and mass spectrometry are used to detect the non-polar analyte. In one embodiment, acequinocyl and/or its derivatives is analyzed using liquid chromatography and tandem mass spectrometry (LC-MS/MS) and the improved LC-MS/MS conditions allows detection limits of acequinocyl and/or its derivatives of 50 ppb or less.


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