The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 31, 2019

Filed:

Apr. 25, 2018
Applicant:

Archer Daniels Midland Company, Decatur, IL (US);

Inventors:

Kenneth Stensrud, Decatur, IL (US);

Chi-Cheng Ma, Forsyth, IL (US);

Kevin Martin, Mt. Zion, IL (US);

Assignee:

ARCHER DANIELS MIDLAND COMPANY, Decatur, IL (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01J 27/00 (2006.01); C07D 307/12 (2006.01); C07C 29/60 (2006.01); C07C 29/132 (2006.01); C07G 3/00 (2006.01); B01J 23/72 (2006.01); B01J 23/46 (2006.01); B01J 25/00 (2006.01); B01J 27/053 (2006.01); B01J 27/16 (2006.01); B01J 27/20 (2006.01);
U.S. Cl.
CPC ...
C07D 307/12 (2013.01); B01J 23/462 (2013.01); B01J 23/72 (2013.01); B01J 25/00 (2013.01); B01J 27/053 (2013.01); B01J 27/16 (2013.01); B01J 27/20 (2013.01); C07C 29/132 (2013.01); C07C 29/60 (2013.01); C07G 3/00 (2013.01);
Abstract

Disclosed herein are methods for synthesizing 1,2,5,6-hexanetetrol (HTO), 1,6 hexanediol (HDO) and other reduced polyols from C5 and C6 sugar alcohols or R glycosides. The methods include contacting the sugar alcohol or R-glycoside with a copper catalyst, most desirably a Raney copper catalyst with hydrogen for a time, temperature and pressure sufficient to form reduced polyols having 2 to 3 fewer hydoxy groups than the starting material. When the starting compound is a C6 sugar alcohol such as sorbitol or R-glycoside of a C6 sugar such as methyl glucoside, the predominant product is HTO. The same catalyst can be used to further reduce the HTO to HDO.


Find Patent Forward Citations

Loading…