The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 17, 2019

Filed:

Mar. 22, 2017
Applicant:

Institute of Metal Research Chinese Academy of Sciences, Shenyang, Liaoning Province, CN;

Inventors:

Songfeng Pei, Shenyang, CN;

Wencai Ren, Shenyang, CN;

Huiming Cheng, Shenyang, CN;

Assignee:

Other;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C01B 32/192 (2017.01); C01B 32/205 (2017.01); C01B 32/23 (2017.01); C01B 32/198 (2017.01); C01B 32/225 (2017.01); B82Y 30/00 (2011.01); B82Y 40/00 (2011.01);
U.S. Cl.
CPC ...
C01B 32/192 (2017.08); C01B 32/198 (2017.08); C01B 32/205 (2017.08); C01B 32/225 (2017.08); C01B 32/23 (2017.08); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01);
Abstract

Provided is a method for continuously preparing graphene oxide nanoplatelets by electrochemical treatment, comprising using a continuous graphite product, successively processing two step treatments, i.e. an electrochemical intercalation and an electrolytic oxidation stripping. The electrochemical intercalation is carried out in a concentrated acid, using a graphite material as an anode and energizing under a soaking condition such that acid radical ions enter into graphite interlamination under the drive of an electric field, to form an intercalated graphite continuous material with first-order or low-order intercalation. The electrolytic stripping is using the intercalated continuous graphite material as an anode, energizing in an aqueous electrolyte solution, and performing oxidation stripping. The method has the following advantages: a product does not contain a metal impurity, the oxidation degree of graphene is controllable, the process is continuable and automatable, and the method is safe and has low emissions, etc.


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