The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 10, 2019

Filed:

Apr. 11, 2017
Applicant:

National Technology & Engineering Solutions of Sandia, Llc, Albuquerque, NM (US);

Inventors:

Dale L. Huber, Albuquerque, NM (US);

John Daniel Watt, Albuquerque, NM (US);

Jonathan Chavez, Grovetown, GA (US);

Lauren Marie Ammerman, Albuquerque, NM (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B22F 9/04 (2006.01); B22F 1/00 (2006.01);
U.S. Cl.
CPC ...
B22F 9/04 (2013.01); B22F 1/0044 (2013.01); B22F 2301/255 (2013.01);
Abstract

The invention provides a green chemistry, aqueous method to synthesize gold nanoparticles directly from bulk gold sources. The method involves the ultrasonication of bulk gold in water in the presence of an alkythiol species and a quaternary ammonium surfactant. An organic bilayer forms on the surface of the gold which renders it susceptible to material ejection from the violent collapse of cavitation bubbles. This ejected material is stabilized in solution by the formation of an organic bilayer and can be easily separated. It can then be subjected to an aqueous digestive ripening step to give a gold nanoparticle ensemble with a well-defined plasmon resonance. This method is applicable to a number of different sources of bulk gold. The method can be applied to an environmentally important problem; the recovery of gold from electronic waste streams. For example, gold nanoparticles can be extracted directly from the surface of SIM cards, with no prior manipulation of the cards necessary.


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