The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 12, 2019

Filed:

Sep. 11, 2016
Applicant:

Nanjing University, Nanjing, CN;

Inventors:

Wei Shi, Nanjing, CN;

Jing Guo, Nanjing, CN;

Hongxia Yu, Nanjing, CN;

Assignee:

Nanjing University, Nanjing, CN;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N 33/50 (2006.01); G06F 16/245 (2019.01); B01D 15/00 (2006.01); G01N 33/74 (2006.01); C12Q 1/00 (2006.01); G06F 19/00 (2018.01);
U.S. Cl.
CPC ...
G01N 33/5014 (2013.01); B01D 15/00 (2013.01); C12Q 1/00 (2013.01); G01N 33/743 (2013.01); G06F 16/245 (2019.01); G06F 19/326 (2013.01);
Abstract

Implementations herein relates to effect-directed identification of targeted and non-targeted androgen disruptors. The implementations include primary separation, androgenic activity testing, high throughput separation and preparation of toxicants, active component scanning based on high performance liquid chromatography-time of flight mass spectrometry, targeted screening of suspicious androgenic substances, non-target identification of androgenic compounds combining mass spectrum, chromatography and toxicity characteristics and toxicity confirmation. The implementations perform separation using SPE and preparative separation in series to obtain high throughput separation fractions, utilize DMSO as a protective agent to optimize concentration of second fractions, utilize target databases to achieve target identification of key toxicants. In addition, assess mass spectrum characteristic identification based on TOF-MS library spectrum, assess chromatography characteristic identification methods based on relationship between retention times and characteristics of compounds, assess toxicity characteristic identification methods based on molecular dynamics simulation techniques, and further assess non-targeted identification and determination of key androgenic substances in the fractions.


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