The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 12, 2019

Filed:

May. 09, 2017
Applicant:

Dow Technology Investments Llc, Midland, MI (US);

Inventors:

Fred A. Conneway, Chonburi, TH;

Clyde L. Rhodes, II, Scott Depot, WV (US);

John F. Szul, Hurricane, WV (US);

Assignee:

Dow Technology Investments LLC, Midland, MI (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B01D 5/00 (2006.01); C07C 31/20 (2006.01); C07D 301/32 (2006.01); B01D 3/04 (2006.01);
U.S. Cl.
CPC ...
B01D 5/0063 (2013.01); B01D 3/04 (2013.01); B01D 5/0012 (2013.01); C07D 301/32 (2013.01); B01D 5/0057 (2013.01); C07C 31/20 (2013.01);
Abstract

Methods, apparatus, and processes are provided for a condenser including flowing a vapor stream including formaldehyde into a tube bundle in a vertical upflow reflux condenser, where a tube in the tube bundle has a length to outside diameter ratio of greater than about 170:1, flowing a cooling fluid on a shell-side of the vertical upflow reflux condenser to condense at least a portion of the vapor stream, where the condensed portion of the vapor stream forms a wetted tube internal surface area on each tube in the generally upright tube bundle; and maintaining the vapor stream velocity at a rate that provides a liquid residence time where formaldehyde condensed on the wetted internal surface area of each tube can react with water to form methylene glycol, removing at least sixty percent (60%) of formaldehyde from the vapor stream fed to the condenser.


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