The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 29, 2019

Filed:

Feb. 18, 2015
Applicant:

Nanotek Instruments, Inc., Dayton, OH (US);

Inventors:

Hui He, Dayton, OH (US);

Aruna Zhamu, Springboro, OH (US);

Bor Z. Jang, Centerville, OH (US);

Assignee:

Nanotek Instruments, Inc., Dayton, OH (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01M 4/36 (2006.01); H01M 4/136 (2010.01); H01M 4/38 (2006.01); H01M 10/0565 (2010.01); H01M 10/0567 (2010.01); H01M 10/0569 (2010.01); H01M 4/46 (2006.01); H01M 10/0525 (2010.01); H01M 10/054 (2010.01); H01M 4/13 (2010.01); H01M 4/58 (2010.01); H01M 10/052 (2010.01); H01M 10/0568 (2010.01); H01M 4/02 (2006.01);
U.S. Cl.
CPC ...
H01M 4/366 (2013.01); H01M 4/13 (2013.01); H01M 4/136 (2013.01); H01M 4/381 (2013.01); H01M 4/382 (2013.01); H01M 4/387 (2013.01); H01M 4/463 (2013.01); H01M 4/5815 (2013.01); H01M 10/052 (2013.01); H01M 10/054 (2013.01); H01M 10/0525 (2013.01); H01M 10/0565 (2013.01); H01M 10/0567 (2013.01); H01M 10/0568 (2013.01); H01M 10/0569 (2013.01); H01M 2004/027 (2013.01); H01M 2004/028 (2013.01); H01M 2300/0025 (2013.01); H01M 2300/0034 (2013.01); H01M 2300/0082 (2013.01);
Abstract

A method of producing a pre-sulfurized active cathode layer for a rechargeable alkali metal-sulfur cell; the method comprising: (a) Preparing an integral layer of meso-porous structure of a carbon, graphite, metal, or conductive polymer having a specific surface area greater than 100 m/g; (b) Preparing an electrolyte comprising a solvent and a sulfur source; (c) Preparing an anode; and (d) Bringing the integral layer and the anode in ionic contact with the electrolyte and imposing an electric current between the anode and the integral layer (serving as a cathode) to electrochemically deposit nano-scaled sulfur particles or coating on the graphene surfaces. The sulfur particles or coating have a thickness or diameter smaller than 20 nm (preferably <10 nm, more preferably <5 nm or even <3 nm) and occupy a weight fraction of at least 70% (preferably >90% or even >95%).


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