The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 29, 2019

Filed:

Sep. 07, 2015
Applicant:

Psc Polysilane Chemicals Gmbh, Bitterfeld-Wolfen, DE;

Inventors:

Christian Bauch, Muldestausee-Ot Muldenstein, DE;

Sven Holl, Gückingen, DE;

Matthias Heuer, Sandersdorf-Brehna Ot Ramsin, DE;

Assignee:

PSC POLYSILANE CHEMICALS GMBH, Bitterfeld-Wolfen, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 33/107 (2006.01); C01B 33/04 (2006.01); B01D 3/34 (2006.01); C01B 33/00 (2006.01); C07F 7/20 (2006.01); C07D 323/00 (2006.01); C08G 77/60 (2006.01); C08K 3/16 (2006.01); C08K 5/54 (2006.01);
U.S. Cl.
CPC ...
C01B 33/10773 (2013.01); B01D 3/34 (2013.01); C01B 33/00 (2013.01); C01B 33/04 (2013.01); C01B 33/10778 (2013.01); C07D 323/00 (2013.01); C07F 7/20 (2013.01); C08G 77/60 (2013.01); C08K 3/16 (2013.01); C08K 5/54 (2013.01);
Abstract

The invention relates to a method for purifying halogenated oligosilanes in the form of a pure compound or a mixture of compounds with respectively at least one direct Si—Si bond, the substituents thereof being exclusively made from halogen or from halogen and hydrogen and in the composition thereof, the atomic ratio of the substituents:silicon is at least 3:2, by the action of at least one purification agent on the halogenated oligosilane and by isolating the halogenated oligosilanes with improved purity. According to prior art, halogenated monosilanes such as HSiClare purified by treating with organic compounds, preferably polymers, containing amino groups, and are separated from said mixtures. Based on the contained amino groups, said method can not be used for halogenated oligosilanes as the secondary reactions lead to a decomposition of the products. The novel method is used to provide the desired products in a high yield and purity without using the amino groups.


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