The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 15, 2019

Filed:

Sep. 25, 2017
Applicant:

Eastman Kodak Company, Rochester, NY (US);

Inventors:

Deepak Shukla, Webster, NY (US);

Kevin M. Donovan, Bergen, NY (US);

Kevin P. Klubek, West Henrietta, NY (US);

Assignee:

EASTMAN KODAK COMPANY, Rochester, NY (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
G03C 1/498 (2006.01); C08B 3/16 (2006.01); C08L 1/12 (2006.01); C08L 1/14 (2006.01); C08L 1/28 (2006.01); C08L 1/32 (2006.01); G03F 7/00 (2006.01); H01B 1/22 (2006.01); C08B 3/06 (2006.01); C07C 31/02 (2006.01); B82Y 40/00 (2011.01); C01G 5/02 (2006.01); C08B 3/08 (2006.01); C08K 3/08 (2006.01);
U.S. Cl.
CPC ...
G03C 1/49809 (2013.01); C08B 3/16 (2013.01); C08L 1/12 (2013.01); C08L 1/14 (2013.01); C08L 1/284 (2013.01); C08L 1/286 (2013.01); C08L 1/32 (2013.01); G03F 7/00 (2013.01); H01B 1/22 (2013.01); B82Y 40/00 (2013.01); C01G 5/02 (2013.01); C07C 31/02 (2013.01); C08B 3/06 (2013.01); C08B 3/08 (2013.01); C08K 2003/0806 (2013.01);
Abstract

A method is used to prepare silver nanoparticles in the form of a silver nanoparticle cellulosic polymeric composite. A cellulosic polymer, organic solvent having a boiling point at atmospheric pressure of 100° C. to 500° C. and a Hansen parameter (δ) equal to or greater than that of the cellulosic polymer, and a nitrogenous base are mixed to form a premix solution. Upon heating the premix solution to a temperature of at least 75° C., a solution of reducible silver ions is added that is equimolar or less in relation to the nitrogenous base. The weight ratio of reducible silver ions to the cellulosic polymer is 5:1 to 50:1. The resulting silver nanoparticle composite is cooled, isolated, and re-dispersed in an organic solvent, providing a non-aqueous silver-containing dispersion comprising the silver nanoparticle cellulosic polymeric composite.


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