The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 15, 2019

Filed:

Sep. 26, 2018
Applicant:

Shin-etsu Chemical Co., Ltd., Tokyo, JP;

Inventors:

Yuki Miyake, Joetsu, JP;

Takeshi Kinsho, Joetsu, JP;

Ryo Komatsu, Joetsu, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/327 (2006.01); C07C 67/24 (2006.01); C07C 69/734 (2006.01); C07C 67/03 (2006.01); C07C 67/303 (2006.01); C07C 67/313 (2006.01); C07C 67/32 (2006.01); C07C 67/343 (2006.01);
U.S. Cl.
CPC ...
C07C 67/327 (2013.01); C07C 67/03 (2013.01); C07C 67/24 (2013.01); C07C 67/303 (2013.01); C07C 67/313 (2013.01); C07C 67/32 (2013.01); C07C 67/343 (2013.01); C07C 69/734 (2013.01); C07B 2200/09 (2013.01);
Abstract

One object of the invention is to provide a method for preparing a 9,9-dialkoxy-7-nonynoate ester and (7E)-7,9-decadienoate ester, which are valuable as intermediates. The method for preparing a (7E)-7,9-decadienoate ester (5) comprises at least steps of: hydrolyzing a 9,9-dialkoxy-7-nonenoate ester (2), RO(RO)CHCH═CH(CH)COR, to form a (7E)-9-oxo-7-nonenoate ester (3); and subjecting the (7E)-9-oxo-7-nonenoate ester (3) to a Wittig reaction with a triarylphosphonium methylide (4), ArP═CH, to form the (7E)-7,9-decadienoate ester (5). The 9,9-dialkoxy-7-nonenoate ester may be prepared by, for example, reducing a 9,9-dialkoxy-7-nonynoate ester (1).


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