The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 03, 2019

Filed:

Oct. 03, 2017
Applicant:

Mitsui Chemicals, Inc., Minato-ku, Tokyo, JP;

Inventors:

Naoyuki Kakinuma, Omuta, JP;

Masayuki Furuya, Arao, JP;

Michiharu Sakata, Kurume, JP;

Koichi Tokunaga, Chikugo, JP;

Shigetoshi Kuma, Kurume, JP;

Assignee:

MITSUI CHEMICALS, INC., Minato-Ku, Tokyo, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 209/26 (2006.01); C07C 211/19 (2006.01); C07C 263/10 (2006.01); B01J 31/24 (2006.01); C07C 255/47 (2006.01); C07C 265/14 (2006.01); C07B 63/00 (2006.01); C07C 253/30 (2006.01); C07C 253/34 (2006.01);
U.S. Cl.
CPC ...
C07C 263/10 (2013.01); B01J 31/24 (2013.01); C07B 63/00 (2013.01); C07C 209/26 (2013.01); C07C 211/19 (2013.01); C07C 253/30 (2013.01); C07C 253/34 (2013.01); C07C 255/47 (2013.01); C07C 265/14 (2013.01); C07C 2602/42 (2017.05);
Abstract

A manufacturing method of an amine compound including obtaining a reaction solution containing an aldehyde compound by reacting a compound represented by Formula (a1) or (a2) with hydrogen and carbon monoxide in the presence of a metal compound of groups 8 to 10 and a phosphorus compound, neutralizing the reaction, purifying an aldehyde compound by distilling the neutralized reaction solution, and reacting the aldehyde compound with ammonia and with hydrogen in the presence of a catalyst to obtain an amine compound, wherein the phosphorus compound is represented by the Formula (RO)P, and the base compound is at least one selected from carbonate and hydrogen carbonate of metals of group I and carbonate and hydrogen carbonate of metals of group II, and wherein the neutralizing the reaction solution is performed within a temperature range of 40° C. to 50° C.


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