The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 27, 2019

Filed:

Mar. 01, 2016
Applicant:

The Hong Kong Research Institute of Textiles and Apparel Limited, Kowloon, HK;

Inventors:

Yunzi Hu, Kowloon, HK;

Carol Sze Ki Lin, Kowloon, HK;

Walid Daoud, Kowloon, HK;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 319/00 (2006.01); C07D 319/12 (2006.01); B01J 23/06 (2006.01); B01J 35/00 (2006.01); B01J 35/10 (2006.01);
U.S. Cl.
CPC ...
C07D 319/12 (2013.01); B01J 23/06 (2013.01); B01J 35/0013 (2013.01); B01J 35/10 (2013.01);
Abstract

The present invention relates to a method for the catalytic synthesis of lactide from lactic acid. The method relates to the synthesis of lactide from lactic acid under the catalysis of a zinc oxide nanoparticle aqueous dispersion as a catalyst. The present invention has four technical characteristics: I. the zinc oxide nanoparticle aqueous dispersion catalyst has a sufficient surface area, and the size of nanoparticles is merely 30-40 nm, providing a sufficient contact area between the substrate (lactic acid) and the catalyst; II. the new catalyst has a milder catalytic effect on polymerization, allowing the molecular weight distribution of a prepolymer within a range of 400-1500 g/mol, which is advantageous for depolymerization to proceed; III. the new catalyst is stable, thus avoiding oxidation or carbonization in a high temperature reaction; and IV. the new catalyst has a low toxicity and a small threat to human health.


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