The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 27, 2019

Filed:

Dec. 21, 2012
Applicant:

The Asan Foundation, Seoul, KR;

Inventors:

Sang Ju Lee, Seoul, KR;

Seung Jun Oh, Seoul, KR;

Dae Hyuk Moon, Seoul, KR;

Jin Sook Ryu, Seoul, KR;

Jae Seung Kim, Seoul, KR;

Jong Jin Lee, Seoul, KR;

Assignee:

THE ASAN FOUNDATION, Seoul, KR;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 303/32 (2006.01); C07B 59/00 (2006.01); C07C 217/80 (2006.01); C07C 309/01 (2006.01); C07D 213/64 (2006.01); C07D 233/91 (2006.01); C07D 451/02 (2006.01); C07H 19/06 (2006.01); C07D 403/06 (2006.01); C07C 213/08 (2006.01); C07D 471/04 (2006.01); C07C 253/30 (2006.01); A61K 51/04 (2006.01);
U.S. Cl.
CPC ...
C07C 303/32 (2013.01); A61K 51/04 (2013.01); A61K 51/0455 (2013.01); C07B 59/00 (2013.01); C07C 213/08 (2013.01); C07C 217/80 (2013.01); C07C 253/30 (2013.01); C07C 309/01 (2013.01); C07D 213/64 (2013.01); C07D 233/91 (2013.01); C07D 403/06 (2013.01); C07D 451/02 (2013.01); C07D 471/04 (2013.01); C07H 19/06 (2013.01); C07B 2200/05 (2013.01);
Abstract

The present invention relates to a method for labelling fluorine-18, which is a radioisotope, and more specifically, to a method for labelling a [F]fluoride in a method for preparing an organic [F]fluoro compound by reacting an alkyl halide or an alkyl sulfonate with a [F]fluoride, wherein a [F]fluoride supported on a quaternary alkyl ammonium polymer support is eluted using a solution containing a metal salt or a quaternary ammonium salt with an adjusted pH, and a base is not additionally used. The present invention enables a labeling reaction without an additional base after precisely reflecting the concentration of a base absolutely necessary for the nucleophilic substitution of a [F]fluoride or eluting a [F]fluoride using a [F]fluoride eluent with an adjusted pH, thereby stably obtaining a [F]fluoride-labelled compound in a high yield, and is thus useful for production of fluorine-18-labelled radioactive medical supplies.


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