The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 27, 2019

Filed:

Dec. 06, 2016
Applicant:

Ube Industries, Ltd., Ube-shi, JP;

Inventors:

Yoshinori Sugimura, Ube, JP;

Kazunori Kurosawa, Ube, JP;

Kazuo Yamato, Ube, JP;

Junichi Kugimoto, Ube, JP;

Joji Kawai, Bangkok, TH;

Wanna Sirisuksukon, Bangkok, TH;

Nantariya Ngamsup, Bangkok, TH;

Assignee:

UBE INDUSTRIES, LTD., Ube-Shi, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 45/53 (2006.01); C07C 35/08 (2006.01); C07C 49/403 (2006.01); C07C 27/00 (2006.01); C07C 29/00 (2006.01); C07C 27/12 (2006.01); C07C 29/54 (2006.01);
U.S. Cl.
CPC ...
C07C 45/53 (2013.01); C07C 27/00 (2013.01); C07C 27/12 (2013.01); C07C 29/00 (2013.01); C07C 29/54 (2013.01); C07C 35/08 (2013.01); C07C 49/403 (2013.01);
Abstract

A method and a system for inexpensively producing a corresponding target ketone and/or alcohol by decomposing hydroperoxide rapidly and with high selectivity using an aqueous alkaline solution and by recovering and recycling alkali. The method includes neutralizing at least a part of a carboxylic acid in the oxidation reaction solution by contacting the oxidation reaction solution with a first alkaline solution including a carbonate of an alkali metal, and separating the reaction mixture into a first oil phase and a first water phase; decomposing the hydroperoxide and the ester compound in the first oil phase by contacting the first oil phase with a second alkaline solution having a higher pH value than the first alkaline solution, and separating the reaction mixture into a second oil phase and a second water phase; and recovering the carbonate of an alkali metal from the first water phase and recycling the carbonate of an alkali metal to the first alkaline solution.


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