The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 27, 2019

Filed:

May. 29, 2018
Applicant:

Kangwon National University University-industry Cooperation Foundation, Gangwon-do, KR;

Inventor:

Young Jun Song, Gangwon-do, KR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01D 15/00 (2006.01); C01D 15/08 (2006.01); C01D 5/04 (2006.01); C01D 7/02 (2006.01); C01D 7/38 (2006.01); H01M 10/54 (2006.01); C01D 7/26 (2006.01);
U.S. Cl.
CPC ...
C01D 15/08 (2013.01); C01D 5/04 (2013.01); C01D 7/02 (2013.01); C01D 7/26 (2013.01); C01D 7/38 (2013.01); H01M 10/54 (2013.01); C01P 2004/64 (2013.01); C01P 2006/80 (2013.01);
Abstract

Disclosed is a method of producing high-purity lithium carbonate and barium sulfate from discarded lithium secondary batteries, including: a first process for producing high-purity lithium phosphate from a discarded battery; and a second process for producing lithium sulfate from the lithium phosphate and producing lithium carbonate and barium sulfate from the lithium sulfate. The second process has steps of (a) producing a liquid mixture of lithium phosphate and sulfuric acid, (b) obtaining lithium sulfate by condensing the liquid mixture, (c) dissolving the lithium sulfate in water or a sodium hydroxide aqueous solution, depositing phosphoric acid as lithium phosphate, and performing solid-liquid separation (d) depositing lithium carbonate and performing solid-liquid separation to obtain lithium carbonate, (e) finely grinding the lithium carbonate and classifying the particles, (f) controlling a particle size and shape by dissolving edges of particles or minute particles, (g) performing solid-liquid separation, and (h) depositing barium sulfate.


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