The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 20, 2019

Filed:

Dec. 13, 2017
Applicant:

National Chung Shan Institute of Science and Technology, Taoyuan, TW;

Inventors:

Chun-Te Wu, Taoyuan, TW;

Kuan-Ting Lai, Taoyuan, TW;

Cheng-Hung Shih, Taoyuan, TW;

Yang-Kuo Kuo, Taoyuan, TW;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 21/082 (2006.01);
U.S. Cl.
CPC ...
C01B 21/082 (2013.01); C01B 21/0828 (2013.01); C01P 2004/32 (2013.01);
Abstract

A method utilizes easily obtained carbon as carbon source for sintering, followed by high energy ball milling process with planetary ball mill for high energy homogenous mixing of the carbon source, solvent and nano-level silicon dioxide powder, along with a high energy ball milling process repeatedly performed using different sized ball mill beads, so as to formulate a spray granulation slurry with the optimal viscosity, to complete the process of micronization of carbon source evenly encapsulated by silicon dioxide powders. The optimal ratio of C/SiOis 1-2.5 to produce a spherical silicon dioxide powder (40-50 μm) evenly encapsulated by the carbon source. The powder is then subjected to a high temperature (1450□) sintering process under nitrogen gas. Lastly, the sintered silicon nitride powder is subjected to homogenizing carbon removal process in a rotational high temperature furnace to complete the fabricating process.


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