The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 30, 2019

Filed:

Dec. 31, 2015
Applicant:

Kaiser Optical Systems Inc., Ann Arbor, MI (US);

Inventor:

Sean J. Gilliam, Monroe, MI (US);

Assignee:

Kaiser Optical Systems, Inc., Ann Arbor, MI (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
G01N 21/95 (2006.01); G01N 21/57 (2006.01); G01N 21/65 (2006.01); G01N 21/88 (2006.01); G01N 33/15 (2006.01); G01N 21/84 (2006.01); A61J 3/00 (2006.01); A61K 9/28 (2006.01);
U.S. Cl.
CPC ...
G01N 21/9508 (2013.01); G01N 21/57 (2013.01); G01N 21/65 (2013.01); G01N 21/8422 (2013.01); G01N 21/8851 (2013.01); G01N 33/15 (2013.01); A61J 3/005 (2013.01); A61K 9/28 (2013.01); A61K 9/2893 (2013.01);
Abstract

Pharmaceutical tablet properties, including surface roughness, gloss and temperature, are determined in real-time using Raman spectroscopy. A plurality of coated pharmaceutical tablets are provided having a distribution of known values of a surface property to be modeled. The Raman spectrum of each coated tablet is acquired to generate a distribution of Raman spectra. A correlative model is then developed based upon the distribution of the acquired Raman spectra relative to the distribution of the known values of the measured property. The Raman spectrum of a pharmaceutical tablet is then acquired during and/or after a coating process, and the value of the surface property of the tablet is determined using the correlative model. The steps associated with model development are carried out off-line, whereas the step or steps associated with acquiring the Raman spectra of the pharmaceutical tablet during (preferable) or after online coating process(es) are carried out on-line using a remote, fiber-coupled probe.


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