The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 09, 2019

Filed:

Dec. 10, 2015
Applicant:

Shin-etsu Chemical Co., Ltd., Tokyo, JP;

Inventors:

Shuichi Miyao, Niigata, JP;

Shigeyoshi Netsu, Niigata, JP;

Assignee:
Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C01B 33/02 (2006.01); C01B 33/035 (2006.01); G01N 23/20 (2018.01); C30B 29/06 (2006.01); C23C 16/24 (2006.01); C30B 13/00 (2006.01); C30B 28/14 (2006.01);
U.S. Cl.
CPC ...
C01B 33/035 (2013.01); C01B 33/02 (2013.01); C23C 16/24 (2013.01); C30B 13/00 (2013.01); C30B 28/14 (2013.01); C30B 29/06 (2013.01);
Abstract

A plate-shaped sample with a cross-section perpendicular to a radial direction of a polycrystalline silicon rod as a principal surface is sampled from a region from a center (r=0) of the polycrystalline silicon rod to R/3. Then, the sample is disposed at a position at which a Bragg reflection from a (111) Miller index plane is detected. In-plane rotation with a rotational angle φ on the sample is performed with a center of the sample as a rotational center such that an X-ray irradiation region defined by a slit performs φ-scanning on the principal surface of the sample to obtain a diffraction chart indicating dependency of a Bragg reflection intensity from the (111) Miller index plane on a rotational angle of the sample. A ratio (S/S) between an area Sof a peak part appearing in the diffraction chart and a total area Sof the diffraction chart is calculated.


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