The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 04, 2019

Filed:

Dec. 06, 2016
Applicant:

Sabic Global Technologies B.v., Bergen op Zoom, NL;

Inventors:

Satish Chandra Pandey, Karnataka, IN;

Gaurav Mediratta, Karnataka, IN;

Alvaro Carrillo, Delmar, NY (US);

Assignee:

SABIC GLOBAL TECHNOLOGIES B.V., Bergen op Zoom, NL;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 37/20 (2006.01); C07C 39/16 (2006.01); H01M 10/6551 (2014.01); H01M 10/613 (2014.01); H01M 10/052 (2010.01); H01M 2/10 (2006.01); H01M 10/0525 (2010.01); H01M 10/0565 (2010.01); H01M 10/0587 (2010.01);
U.S. Cl.
CPC ...
C07C 37/20 (2013.01); C07C 39/16 (2013.01); H01M 2/1077 (2013.01); H01M 10/052 (2013.01); H01M 10/0525 (2013.01); H01M 10/0565 (2013.01); H01M 10/0587 (2013.01); H01M 10/613 (2015.04); H01M 10/6551 (2015.04); C07C 2527/03 (2013.01); H01M 2300/0065 (2013.01); Y02T 10/7011 (2013.01);
Abstract

An improved method of manufacture of a bisphenol comprises heating a monohydric phenol to a first temperature sufficient to melt the monohydric phenol; adding a carbonyl compound to 2.0-3.0 molar equivalents, based on the moles of carbonyl compound, of the monohydric phenol in the presence of catalytic amounts of an organosulfonic acid catalyst and a reaction promoter at a second temperature sufficient to maintain unreacted monohydric phenol in a molten state; increasing the temperature to a third temperature higher than the second temperature, and mixing for a time sufficient to produce the bisphenol in a yield of 80 to 100%, based on the amount of carbonyl compound; wherein mineral acids, Lewis acids, and ion exchange resins are not used. The method is applicable to the manufacture of 2,2-bis(3,5-dimethyl-4-hydroxyphenyl)propane, a useful intermediate for the manufacture of bi-functional poly(phenylene ether)s.


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