The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 21, 2019

Filed:

Jan. 15, 2015
Applicant:

Shin-etsu Chemical Co., Ltd., Tokyo, JP;

Inventors:

Masami Kaneyoshi, Echizen, JP;

Masatoshi Ishii, Echizen, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C09K 11/61 (2006.01); C01G 19/00 (2006.01); C01G 23/00 (2006.01); C01G 25/00 (2006.01); C01G 27/00 (2006.01); C01G 17/00 (2006.01); C09K 11/67 (2006.01);
U.S. Cl.
CPC ...
C09K 11/617 (2013.01); C01G 17/006 (2013.01); C01G 19/006 (2013.01); C01G 23/002 (2013.01); C01G 25/006 (2013.01); C01G 27/006 (2013.01); C09K 11/675 (2013.01); C01P 2002/50 (2013.01); C01P 2002/54 (2013.01); C01P 2002/84 (2013.01); C01P 2004/61 (2013.01);
Abstract

Provided is a method for producing a phosphor having a chemical composition represented by formula (I), AMF:Mn (I) (A is one type or more of an alkali metal selected from Li, Na, K, Rb, and Cs, and includes at least Na and/or K, and M is one type or more of a tetravalent element selected from Si, Ti, Zr, Hf, Ge, and Sn.), the method comprising preparing a first hydrofluoric acid solution containing M and a second hydrofluoric acid solution containing A as well as either dissolving a compound containing Mn in either the first hydrofluoric acid solution or the second hydrofluoric acid solution or preparing a separate solution in which the compound containing Mn is dissolved. When the solutions are mixed to precipitate the phosphor of the formula (I), the solutions are mixed so that the concentration of M is 0.1 to 0.5 mol/liter when all the solutions are mixed. According to the present invention, a complex fluoride phosphor having excellent luminescence properties can be produced stably with high yield.


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