The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 21, 2019

Filed:

Jun. 24, 2016
Applicant:

Shanghai Forefront Pharmaceutical Co., Ltd, Shanghai, CN;

Inventors:

Wei Li, Shanghai, CN;

Yi Ren, Shanghai, CN;

Chengjun Huang, Shanghai, CN;

Yanyan Zhu, Shanghai, CN;

Shaojun Fu, Shanghai, CN;

Gang Fu, Shanghai, CN;

Zhewen Wei, Shanghai, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 403/14 (2006.01); A61P 31/14 (2006.01); A61K 31/4439 (2006.01);
U.S. Cl.
CPC ...
C07D 403/14 (2013.01); A61K 31/4439 (2013.01); A61P 31/14 (2018.01); C07B 2200/13 (2013.01);
Abstract

The present invention relates to a novel Ledipasvir (LDV) crystal form and a preparation method thereof. Specifically, disclosed is an LDV solvate. The solvate is a solvate formed by LDV and a solvent A and/or a solvent B, wherein the solvent A is acetonitrile or acetone; and the solvent B is methyl tertiary butyl ether (MTBE). Also disclosed are a preparation method and an application of the solvate. The solvate has a high purity, a good crystallization property, and better optical stability. The preparation method is simple and the process is stable. The solvate can significantly improve quality control and industrial applications of LDV-containing drugs.


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