The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 14, 2019

Filed:

Oct. 12, 2017
Applicant:

The United States of America, As Represented BY the Secretary of the Navy, Washington, DC (US);

Inventors:

Michael E. Wright, Ridgecrest, CA (US);

Benjamin G. Harvey, Ridgecrest, CA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 253/04 (2006.01); C07C 37/00 (2006.01); C07C 37/16 (2006.01); C12P 13/00 (2006.01); C08G 65/38 (2006.01); D06M 13/345 (2006.01); D06M 101/40 (2006.01);
U.S. Cl.
CPC ...
C07C 253/04 (2013.01); C07C 37/002 (2013.01); C07C 37/003 (2013.01); C07C 37/16 (2013.01); C08G 65/38 (2013.01); C12P 13/002 (2013.01); D06M 13/345 (2013.01); D06M 2101/40 (2013.01);
Abstract

A method for converting vanillin to bis(cyanate) ester monomers, comprising treating vanillin with a reductive coupling agent to form at least one olefin. The olefin or olefins are treated with hydrogen and a metal catalyst to hydrogenate said olefin. The hydrogenated olefin or olefins are treated with at least one cyanogen halide and a base in an organic solvent to afford at least one olefin monomer. The olefin monomer or monomers are purified by recrystallization or precipitation from an organic solvent.


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