The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 30, 2019

Filed:

Jul. 06, 2015
Applicant:

K.d. Pharma Bexbach Gmbh, Bexbach, DE;

Inventor:

Rudolf Krumbholz, Merchweiler, DE;

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C11B 7/00 (2006.01); B01D 3/14 (2006.01); B01D 1/06 (2006.01); B01D 3/12 (2006.01); C07C 67/54 (2006.01); C11B 3/12 (2006.01); C11C 1/00 (2006.01); C11C 1/02 (2006.01); B01D 3/10 (2006.01); B01D 5/00 (2006.01); C07C 69/587 (2006.01);
U.S. Cl.
CPC ...
C11B 7/00 (2013.01); B01D 1/065 (2013.01); B01D 3/10 (2013.01); B01D 3/12 (2013.01); B01D 3/148 (2013.01); B01D 5/0045 (2013.01); C07C 67/54 (2013.01); C11B 3/12 (2013.01); C11C 1/002 (2013.01); C11C 1/005 (2013.01); C11C 1/02 (2013.01); C07C 69/587 (2013.01); C11B 7/0075 (2013.01);
Abstract

A process for obtaining free fatty acid and/or free fatty acid ester, including separating a liquid mixture containing the free fatty acid and/or the fatty acid ester by contacting a vapor of the liquid mixture in a column of a distillation apparatus with condensate formed from the vapor running downward. Heat and mass transfer takes place between the vapor and the condensate on column internals. The column has at least 10 theoretical plates and the separation is conducted with a pressure drop between the top and bottom of the column of Δp of ≥3.3 mbars. Appropriately, the liquid mixture, contains polyunsaturated fatty acid, preferably omega-6 or omega-3 fatty acid and/or alkyl monoesters and/or glycerol monoesters. In one embodiment the column has at least 30 theoretical plates and the separation is conducted with a pressure drop Δp between 3.5 mbar and 6 mbar.


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