The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 23, 2019

Filed:

Aug. 19, 2015
Applicant:

Forschungszentrum Juelich Gmbh, Juelich, DE;

Inventors:

Qianli Ma, Juelich, DE;

Frank Tietz, Monschau, DE;

Olivier Guillon, Juelich, DE;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01M 10/05 (2010.01); C01B 25/45 (2006.01); H01M 10/0562 (2010.01); H01M 10/052 (2010.01); H01M 10/0525 (2010.01); H01M 12/08 (2006.01);
U.S. Cl.
CPC ...
H01M 10/0562 (2013.01); C01B 25/45 (2013.01); H01M 10/052 (2013.01); H01M 10/0525 (2013.01); H01M 12/08 (2013.01); C01P 2006/40 (2013.01); H01M 2300/0065 (2013.01); H01M 2300/0068 (2013.01);
Abstract

A method for preparing a lithium titanium phosphate, wherein a sol-gel process is used to prepare the phosphate, includes producing a sol from source materials; converting the sol to a gel; and drying the gel to obtain a corresponding powder comprising the lithium titanium phosphate. In a substep, the method further includes adding titanium(IV) isopropoxide to water to produce precipitates of titanium hydroxide oxide, cooling a system down to a temperature of less than 10° C., and redissolving the precipitates by adding nitric acid to form an aqueous TiOnitrate solution. The lithium titanium phosphate has a general composition LiMTi(PO)(SiO), wherein M=Al, Ga, In, Sc, V, Cr, Mn, Co, Fe, Y, La—Lu, wherein 0≤x≤0.5, and wherein 0≤y≤0.5.


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