The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 23, 2019

Filed:

Apr. 05, 2016
Applicant:

Shell Oil Company, Houston, TX (US);

Inventors:

Pieter Huizenga, Amsterdam, NL;

Kai Jürgen Fischer, Amsterdam, NL;

Karin Bus, Amsterdam, NL;

Waldo Eugene De Villiers, Katy, TX (US);

Carmelo Perez Golf, Amsterdam, NL;

Assignee:

SHELL OIL COMPANY, Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/82 (2006.01); C07C 29/80 (2006.01); C07C 31/20 (2006.01);
U.S. Cl.
CPC ...
C07C 29/82 (2013.01); C07C 29/80 (2013.01);
Abstract

The invention provides a process for the separation of MEG and 1,2-BDO from a first mixture comprising MEG and 1,2-BDO in a weight ratio of at least 10:1 (MEG:1,2-BDO), said process comprising the steps of; (i) providing the first mixture as a feed to a distillation column at a point in the range of from 20 to 80% of the column height; (ii) operating the distillation at a temperature in the range of from 120 to 190° C. and at a pressure in the range of from 5 kPa to atmospheric pressure; (iii) removing an MEG stream from the distillation column at a point below the point at which the first mixture is fed; (iv) removing an overheads stream comprising an azeotrope of MEG and 1,2-BDO.


Find Patent Forward Citations

Loading…