The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 23, 2019

Filed:

Jun. 08, 2015
Applicant:

Battelle Memorial Institute, Richland, WA (US);

Inventor:

Wei Liu, Richland, WA (US);

Assignee:

Battelle Memorial Institute, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D 71/02 (2006.01); B01D 69/10 (2006.01); B01D 67/00 (2006.01); B01D 39/20 (2006.01); B01D 69/06 (2006.01); B22F 5/00 (2006.01); C22C 19/00 (2006.01); C22C 19/03 (2006.01); C22C 38/08 (2006.01);
U.S. Cl.
CPC ...
B01D 71/028 (2013.01); B01D 39/2051 (2013.01); B01D 67/0041 (2013.01); B01D 67/0046 (2013.01); B01D 67/0058 (2013.01); B01D 67/0069 (2013.01); B01D 69/06 (2013.01); B01D 69/10 (2013.01); B01D 71/022 (2013.01); B22F 5/006 (2013.01); C22C 19/002 (2013.01); C22C 19/03 (2013.01); C22C 38/08 (2013.01); B01D 2239/10 (2013.01); B01D 2239/1216 (2013.01); B01D 2323/02 (2013.01); B01D 2323/08 (2013.01); B01D 2323/18 (2013.01); B01D 2325/10 (2013.01); B01D 2325/12 (2013.01); B01D 2325/20 (2013.01); B01D 2325/24 (2013.01); B01D 2325/36 (2013.01); B22F 2998/10 (2013.01); Y10T 428/12014 (2015.01); Y10T 428/31678 (2015.04);
Abstract

Zeolite membrane sheets for separation of mixtures containing water are provided, as well as methods for making the same. Thin, but robust, zeolite membrane sheets having an inter-grown zeolite crystal film directly on a thin, less than 200 micron thick, porous support sheet free of any surface pores with a size above 10 microns. The zeolite membrane film thickness is less than about 10 microns above the support surface and less than about 5 microns below the support surface. Methods of preparing the membrane are disclosed which include coating of the support sheet surface with a seed coating solution containing the parent zeolite crystals with mean particle sizes from about 0.5 to 2.0 microns at loading of 0.05-0.5 mg/cm2 and subsequent growth of the seeded sheet in a growth reactor loaded with a growth solution over a temperature range of about 45° C. to about 120° C.


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