The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 16, 2019

Filed:

Dec. 06, 2016
Applicant:

China Jiliang University, Hangzhou, Zhejiang, CN;

Inventors:

Shiqing Xu, Zhejiang, CN;

Huanping Wang, Zhejiang, CN;

Ren Gao, Zhejiang, CN;

Qingong Zhu, Zhejiang, CN;

Qinghua Yang, Zhejiang, CN;

Hellmut Eckert, Zhejiang, CN;

Xianghua Zhang, Zhejiang, CN;

Assignee:

China Jiliang University, Hangzhou, Zhejiang, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C03B 1/00 (2006.01); C03C 13/00 (2006.01); C03B 37/02 (2006.01); C03C 1/02 (2006.01); C03B 19/06 (2006.01); C03B 19/09 (2006.01); C03B 19/10 (2006.01);
U.S. Cl.
CPC ...
C03C 13/00 (2013.01); C03B 1/00 (2013.01); C03B 19/06 (2013.01); C03B 19/09 (2013.01); C03B 19/1065 (2013.01); C03B 37/02 (2013.01); C03C 1/02 (2013.01); C03C 2213/00 (2013.01);
Abstract

A high strength glass fiber is prepared by following steps: weighing raw materials according to a mass percentage of 50-60% silica sol, 24-31% aluminum sol, 8-11% magnesia, 4-5% calcium oxide, 0.1-2% titanium dioxide, 0-0.5% ferric oxide, 0.5-2% niobium pentoxide, 0.5-1.5% antimony trioxide, 0.3-1.5% bismuth nitrate, and 0.1-0.5% boric acid. Deionized water is added. The raw material undergoes mixing by ball milling, spray-drying, calcining, isostatic pressing, melting, and wire-drawing. The invention adopts silicon sol, aluminum sol and bismuth nitrate. Through ball milling and spray-drying, silicon aluminum barium plasmas is evenly coated on surface of other oxide powders. Then nano particles, of silica, alumina and bismuth oxide are obtained by calcining. Under the effect of the high specific surface energy of nano particles, and the close contact of each component, high strength glass fiber is obtained in relatively low fiber drawing temperature while the glass melting temperature and time are significantly reduced.


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