The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 05, 2019

Filed:

Feb. 03, 2016
Applicant:

Evonik Degussa Gmbh, Essen, DE;

Inventors:

Jürgen Stock, Frankfurt, DE;

Joao André, BA Maastricht, NL;

Sebastian Imm, Bad Vilbel, DE;

Matthias Pascaly, Frankfurt, DE;

Assignee:

Evonik Degussa GmbH, Essen, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 301/12 (2006.01); C07D 303/02 (2006.01); B01D 61/02 (2006.01); B01J 23/34 (2006.01); C07C 11/04 (2006.01); C07C 11/06 (2006.01); C07C 21/067 (2006.01);
U.S. Cl.
CPC ...
C07D 301/12 (2013.01); B01D 61/027 (2013.01); C07D 303/02 (2013.01); B01J 23/34 (2013.01); C07C 11/04 (2013.01); C07C 11/06 (2013.01); C07C 21/067 (2013.01);
Abstract

In the method for the epoxidation of an olefin, the olefin is continuously reacted with hydrogen peroxide in a mixed reactor in the presence of a water soluble epoxidation catalyst, comprising a manganese complex, the reaction is carried out in a reaction mixture comprising an aqueous liquid phase and an organic liquid phase with mixing of the liquid phases, reaction mixture is continuously withdrawn from the mixed reactor and separated into a separated aqueous phase and a separated organic phase, and part of the separated aqueous phase is continuously recycled into the mixed reactor, with the combined hold-up time of aqueous phase in withdrawing, separating phases and recycling aqueous phase being kept at less than 15 minutes.


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