The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 27, 2018

Filed:

Aug. 08, 2014
Applicant:

Mitsubishi Gas Chemical Company, Inc., Chiyoda-ku, JP;

Inventors:

Hiroshi Hasegawa, Ibaraki, JP;

Yukako Kozawa, Ibaraki, JP;

Motoharu Takeuchi, Ibaraki, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 15/023 (2006.01); C07C 29/143 (2006.01); B01J 23/86 (2006.01); B01J 29/00 (2006.01);
U.S. Cl.
CPC ...
C01B 15/023 (2013.01); B01J 23/868 (2013.01); B01J 29/00 (2013.01); C07C 29/143 (2013.01); Y02P 20/584 (2015.11); Y02P 20/588 (2015.11);
Abstract

In the production of hydrogen peroxide, when ketone forms are increased upon conversion from higher alcohol components in organic solvents, such increased levels of ketone forms reduce the water content in a working solution and lead to deterioration of catalytic activity. Moreover, increased levels of ketone forms reduce the solubility of anthrahydroquinone compounds and may cause an obstacle to stable and safe operation in the production of hydrogen peroxide due to crystallization and deposition of the anthrahydroquinone compounds. The object of the present invention is to provide a process in which polar solvent-derived altered substances (ketone forms) in a working solution provided for use in the production of hydrogen peroxide via the anthraquinone process are regenerated into the original alcohol components to thereby improve the production efficiency of hydrogen peroxide. From a working solution which has been used for many years, organic solvent components containing ketone forms are separated by distillation and hydrogenated in the presence of a metal catalyst to regenerate the organic solvent components into the original alcohol components, whereby hydrogen peroxide can be produced more efficiently.


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