The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 16, 2018

Filed:

Apr. 04, 2016
Applicant:

Celanese International Corporation, Irving, TX (US);

Inventors:

Ronald D. Shaver, Houston, TX (US);

Yaw-Hwa Liu, Missouri City, TX (US);

Mark O. Scates, Houston, TX (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/12 (2006.01); C07C 51/44 (2006.01); C07C 41/01 (2006.01); B01J 31/20 (2006.01); B01J 31/26 (2006.01); B01J 27/20 (2006.01); B01D 3/00 (2006.01);
U.S. Cl.
CPC ...
C07C 51/12 (2013.01); B01D 3/009 (2013.01); B01J 27/20 (2013.01); B01J 31/20 (2013.01); B01J 31/26 (2013.01); C07C 41/01 (2013.01); C07C 51/44 (2013.01); B01J 2231/34 (2013.01);
Abstract

A process for producing acetic acid is disclosed in which the methyl iodide concentration is maintained in the vapor product stream formed in a flashing step. The methyl iodide concentration in the vapor product stream ranges from 24 to less than 36 wt. % methyl iodide, based on the weight of the vapor product stream. In addition, the acetaldehyde concentration is maintained within the range from 0.005 to 1 wt. % in the vapor product stream. The vapor product stream is distilled in a first column to obtain an acetic acid product stream comprising acetic acid and up to 300 wppm hydrogen iodide and/or from 0.1 to 6 wt. % methyl iodide and an overhead stream comprising methyl iodide, water and methyl acetate.


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