The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 16, 2018

Filed:

Jul. 14, 2015
Applicants:

Research Institute of Shaanxi Yanchang Petroleum (Group) Co., Ltd, Xi'an, Shaanxi, CN;

Dalian University of Technology, Dalian, Liaoning Province, CN;

Inventors:

Wei Zhang, Xi'an, CN;

Xiongfu Zhang, Xi'an, CN;

Dapeng Li, Xi'an, CN;

Ruimin Gao, Xi'an, CN;

Yongbin Lu, Xi'an, CN;

Shuqin Zhang, Xi'an, CN;

Mingfeng Wang, Xi'an, CN;

Pengju Huo, Xi'an, CN;

Si Li, Xi'an, CN;

Chengda Wang, Xi'an, CN;

Weiwu Xu, Xi'an, CN;

Yuan Zhang, Xi'an, CN;

Zhiling Liu, Xi'an, CN;

Ting Pei, Xi'an, CN;

Hua Zhang, Xi'an, CN;

Gang Chen, Xi'an, CN;

Haiou Liu, Xi'an, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 39/40 (2006.01); B01J 29/40 (2006.01);
U.S. Cl.
CPC ...
C01B 39/40 (2013.01); B01J 29/40 (2013.01); C01P 2002/60 (2013.01); C01P 2002/72 (2013.01); C01P 2004/03 (2013.01); C01P 2004/60 (2013.01); C01P 2004/62 (2013.01);
Abstract

A rapid synthesis method of a small-crystal-grain ZSM-5 molecular sieve, the method comprising: preparing a mixed silicon-aluminum glue solution, placing the solution in a crystallization kettle for low-temperature nucleation, enabling high-temperature crystallization growth of the solution, and obtaining a crystallization product, namely, a small-crystal-grain ZSM-5 molecular sieve, the nucleation temperature being 60-120° C., nucleation time being 1-3 hours, a crystallization growth temperature being 150-170° C., and crystallization growth time being 1-3 hours. The method is easy to operate, and has a short operation time, thus being able to complete within 6 hours; in addition, the product has uniform grain sizes, is in a mono-dispersed state, and has a high crystallization degree to a submicron degree.


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