The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 18, 2018

Filed:

Mar. 10, 2016
Applicant:

Carbo Ceramics Inc., Houston, TX (US);

Inventors:

Benjamin T. Eldred, Houston, TX (US);

Brett A. Wilson, Cypress, TX (US);

Clayton F. Gardinier, Houston, TX (US);

Robert Duenckel, Colorado Springs, CO (US);

Todd Roper, Katy, TX (US);

Assignee:

CARBO Ceramics Inc., Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C04B 35/63 (2006.01); C04B 35/64 (2006.01); C09K 8/80 (2006.01); C04B 33/04 (2006.01); C04B 33/32 (2006.01); C04B 35/111 (2006.01); C04B 35/634 (2006.01); C04B 35/636 (2006.01); C04B 35/626 (2006.01); C04B 35/632 (2006.01);
U.S. Cl.
CPC ...
C09K 8/80 (2013.01); C04B 33/04 (2013.01); C04B 33/32 (2013.01); C04B 35/1115 (2013.01); C04B 35/6263 (2013.01); C04B 35/62655 (2013.01); C04B 35/62695 (2013.01); C04B 35/632 (2013.01); C04B 35/634 (2013.01); C04B 35/636 (2013.01); C04B 35/63424 (2013.01); C04B 35/64 (2013.01); C04B 2235/3206 (2013.01); C04B 2235/3208 (2013.01); C04B 2235/3213 (2013.01); C04B 2235/3217 (2013.01); C04B 2235/3272 (2013.01); C04B 2235/349 (2013.01); C04B 2235/444 (2013.01); C04B 2235/94 (2013.01);
Abstract

A method for making proppant particles is provided. The method can include providing a slurry of ceramic raw material, the slurry containing a reactant including a polycarboxylic acid, and flowing the slurry through a nozzle in a gas while vibrating the slurry to form droplets. The method can also include receiving the droplets in a vessel containing a liquid having an upper surface in direct contact with the gas, the liquid containing a coagulation agent. The method can further include reacting the reactant with the coagulation agent to cause coagulation of the reactant in the droplets. The droplets can then be transferred from the liquid and dried to form green pellets. The method can include sintering the green pellets in a selected temperature range to form the proppant particles. In one or more exemplary embodiments, the reactant can be or include a PMA:PAA copolymer.


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