The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 10035744 B1

PDF
Full Text
Expired
Date of Patent:
Jul. 31, 2018

Filed:

Nov. 04, 2015
Applicant:

Shell Oil Company, Houston, TX (US);

Inventors:

Pieter Huizenga, Amsterdam, NL;

Kai Jürgen Fischer, Amsterdam, NL;

Waldo Eugene De Villiers, Katy, TX (US);

Karin Bus, Amsterdam, NL;

Dorien Veldhuizen, Amsterdam, NL;

Assignee:

SHELL OIL COMPANY, Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/86 (2006.01); B01D 11/00 (2006.01); B01D 11/04 (2006.01);
U.S. Cl.
CPC ...
C07C 29/86 (2013.01); B01D 11/0426 (2013.01); B01D 11/0492 (2013.01); B01D 2011/002 (2013.01);
Abstract

The invention provides a process for the separation of MEG and 1,2-BDO from a first mixture comprising MEG and 1,2-BDO in a first solvent by the steps of: (i) combining said first mixture with a second solvent stream comprising a second solvent in a first extraction column; (ii) recovering (a) a second mixture of MEG and 1,2-BDO in the second solvent, wherein the molar ratio of MEG:1,2-BDO is lower in the second mixture than in the first mixture; and (b) a solution comprising MEG in the first solvent; (iii) combining said second mixture with a first washing stream, said first washing stream also comprising the first solvent in a second extraction column; (iv) recovering (c) a first extract stream comprising the second solvent and 1,2-BDO and (d) a third mixture comprising MEG and, optionally, 1,2-BDO in the first solvent.


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