The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 10, 2018

Filed:

Jul. 13, 2017
Applicant:

Archer Daniels Midland Company, Decatur, IL (US);

Inventors:

Brennan Smith, Decatur, IL (US);

ChiCheng Ma, Forsyth, IL (US);

Assignee:

Archer Daniels Midland Company, Decatur, IL (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/76 (2006.01); B01D 1/00 (2006.01); C07D 307/20 (2006.01); C07C 29/58 (2006.01); B01D 15/36 (2006.01); B01D 15/18 (2006.01); B01D 1/22 (2006.01);
U.S. Cl.
CPC ...
C07C 29/76 (2013.01); B01D 1/22 (2013.01); B01D 15/185 (2013.01); B01D 15/361 (2013.01); C07C 29/58 (2013.01); C07D 307/20 (2013.01);
Abstract

A method of isolating and purifying a product of sugar alcohol or anhydrosugar alcohol hydrogenolysis from a reaction mixture containing sorbitans, 1,2,4-butanetriol (BTO), 1,2,5,6-hexanetetrol (HTO), among other byproducts of a hydrogenolysis reaction of a sugar alcohol and/or a mono- or di-dehydrative product of a sugar alcohol is described. The method involves contacting the mixture having the products of sugar alcohol or anhydrosugar alcohol hydrogenation and other C-Calcohols and polyols with a resin material adapted for chromatography under conditions where the products preferentially associates with the resin relative to other components in the mixture, and eluting products from the resin with a solvent. The method suggests a way for separation of aliphatic polyols generated from the hydrogenolysis of sugar alcohols or anhydrosugar alcohols.


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