The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 10, 2018

Filed:

Jul. 23, 2014
Applicant:

Shanghai Wuzheng Engineering Technology Co., Ltd., Shanghai, CN;

Inventors:

Baoming Wang, Shanghai, CN;

Donghui Wang, Shanghai, CN;

Yujiang Li, Shanghai, CN;

Changqing Xu, Shanghai, CN;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 67/00 (2006.01); C07C 29/151 (2006.01); C07C 67/36 (2006.01); B01J 8/02 (2006.01);
U.S. Cl.
CPC ...
C07C 29/151 (2013.01); B01J 8/02 (2013.01); B01J 8/0278 (2013.01); C07C 67/36 (2013.01); B01J 2208/027 (2013.01);
Abstract

A method and a device system for producing dimethyl oxalate through high-pressure carbonylation of industrial synthesis gases and producing ethylene glycol through dimethyl oxalate hydrogenation. The method comprises the following steps: adopting industrial NO, Oand methanol as raw materials to perform an esterification reaction to produce methyl nitrite, then adopting industrial CO and methyl nitrite to perform a carbonylation reaction in a plate reactor to produce carbonylation products which mainly include dimethyl oxalate and dimethyl carbonate, separating the carbonylation products to obtain dimethyl carbonate products, and subsequently performing hydrogenation to dimethyl oxalate in the plate reactor to produce ethylene glycol products; and performing coupling recovery treatment to waste acid in the esterification reaction and purge gas in the carbonylation reaction for recycling. The system comprises an esterification reaction system, a carbonylation reaction system, a purge gases and waste acid coupling recovery system and a hydrogenation reaction system.


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