The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 03, 2018

Filed:

Oct. 10, 2016
Applicant:

Ut-battelle, Llc, Oak Ridge, TN (US);

Inventors:

Jaswinder K. Sharma, Oak Ridge, TN (US);

Panos G. Datskos, Knoxville, TN (US);

Assignee:

Other;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
D01F 9/10 (2006.01); B01J 19/10 (2006.01); C01B 33/12 (2006.01); C01B 33/023 (2006.01);
U.S. Cl.
CPC ...
D01F 9/10 (2013.01); B01J 19/10 (2013.01); C01B 33/023 (2013.01); C01B 33/12 (2013.01); B01J 2219/08 (2013.01); B01J 2219/0877 (2013.01); D10B 2101/02 (2013.01); Y10T 428/298 (2015.01);
Abstract

A method for synthesizing silica nanofibers using sound waves is provided. The method includes providing a solution of polyvinyl pyrrolidone, adding sodium citrate and ammonium hydroxide to form a first mixture, adding a silica-based compound to the solution to form a second mixture, and sonicating the second mixture to synthesize a plurality of silica nanofibers having an average cross-sectional diameter of less than 70 nm and having a length on the order of at least several hundred microns. The method can be performed without heating or electrospinning, and instead includes less energy intensive strategies that can be scaled up to an industrial scale. The resulting nanofibers can achieve a decreased mean diameter over conventional fibers. The decreased diameter generally increases the tensile strength of the silica nanofibers, as defects and contaminations decrease with the decreasing diameter.


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