The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 26, 2018

Filed:

Feb. 05, 2016
Applicant:

The United States of America As Represented BY the Secretary of Agriculture, Washington, DC (US);

Inventors:

JunYong Zhu, Madison, WI (US);

Liheng Chen, Madison, WI (US);

Rolland Gleisner, Jefferson, WI (US);

Assignee:

Other;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
D21B 1/06 (2006.01); C08B 15/08 (2006.01); D21C 9/00 (2006.01); D21B 1/02 (2006.01);
U.S. Cl.
CPC ...
D21B 1/021 (2013.01); C08B 15/08 (2013.01); D21B 1/06 (2013.01); D21C 9/005 (2013.01); D21C 9/007 (2013.01);
Abstract

Methods for integrating the production of carboxylated CNCs and carboxylated CNFs from cellulose are provided. Carboxylated CNCs, carboxylated cellulosic solid residues (CSRs) in the form of cellulose fibers (CF) and/or cellulose microfibrils (CMFs), and carboxylated CNFs fabricated using the methods are also provided. The methods are based on the acid hydrolysis of a cellulosic material using weak solid organic acids to produce carboxylated CNCs and CNFs with thermal stabilities that are higher than the thermal stabilities of the cellulosic materials from which they are derived.


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