East China University of Science and Technology

Luoyang Petrochemical Engineering Corporation (lpec) Sinopec

Sinopec Zhenhai Refining & Chemical Company Limited

Shanghai Huachang Environment Protection Co., Ltd.

Zhuoqun Qian

Hualin Wang

Yanhong Zhang

Ji Ma

Ping Zhou

Qiang Yang

Zhishan Bai

Xin Cui

Liquan Li

Qian Zeng

Chonggang Chen

Jianwen Wang

Chengyu Xu

Tianming Hou

Hejie Li

Jianghua Xu

Lixin Zhang

Xiaomei Xu

Baohua Dai

Jiangqing Hu

Shuilong Yu

The invention relates to a short-flow process for desulfurization of circulating hydrogen and a device for the same. A short-flow process for desulfurization of circulating hydrogen is provided, comprising: (a) removing hydrocarbons from the circulating hydrogen mixture, so that the liquid drops of the heavy hydrocarbons in the dispersion phase are separated from the circulating hydrogen in the continuous phase, and a heavy hydrocarbon phase and a mixture phase of circulating hydrogen containing sulfur are obtained; (b) further separating the resultant mixture phase to remove the sulfides therein, so that circulating hydrogen without sulfur is obtained; (c) further separating the resultant circulating hydrogen without sulfur to remove the amine solution therein, so that purified circulating hydrogen is obtained. The invention also provides a device for desulfurization of circulating hydrogen.

Short-flow process for desulfurization of circulating hydrogen and device for the same

A process and an apparatus for separating and recovering waste alkali from a cyclohexane oxidation solution are provided. A gradient combination of the gravity separation technique, the vortex separation technique and the coalescence separation technique is used to carry out fine separation of the waste alkali liquor from the cyclohexane oxidation solution. The purified cyclohexane oxidation solution is fed into a down-stream apparatus. Most of the waste alkali liquor thus separated is recycled, while the remaining is expelled. The expelled waste alkali liquor is incinerated in an incinerator, followed by recovering the molten species using a pneumatic pulverization process.

Process and apparatus for separating and recovering waste alkali from cyclohexane oxidation solution

The present invention falls within the field of purifying oil-laden wastewater, which provides a method for purifying coke-cooling wastewater in a delayed coking process in petroleum chemical field. The method comprises the following steps: (a) cooling the coke-cooling wastewater produced in a delayed coking process to 5-55&#xb0; C. under 0.1-0.25 MPa absolute pressure, to obtain cooled coke-cooling wastewater; (b) subjecting the cooled coke-cooling wastewater to solid-liquid separation, to obtain a coke breeze phase and a liquid phase; (c) further separating the obtained liquid phase, to obtain an oil phase and a water phase; and (d) further discharging water from the obtained oil phase, to obtain the separated oil phase. The present invention also provides an equipment for carrying out the method. The method of the present invention has the following advantages: low cost for the equipment, good effect for treating coke-cooling wastewater, effectively preventing sulfur pollution and foul odor pollution, saving resources and improving the overall utility of the resources, and improving the cool coking efficiency.

Treating method and equipment for coke-cooling wastewater

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Shanghai, China

Zhuoqun Qian