China University of Geosciences (wuhan)

Zhaochu Hu

Wen Zhang

Ming Li

Tao He

Haihong Chen

Yongsheng Liu

The present invention provides an analysis method for determining halogens in geological samples by ICP-MS. The method includes following steps: weighing a geological sample and ammonium bifluoride in a sample dissolving tank, tightening the sample dissolving tank, and shaking; then heating the sample dissolving tank in a drying oven, and setting a temperature of the drying oven as 200-220&#xb0; C. and heating time as 1-2 hours; cooling the sample dissolving tank to room temperature so as to obtain a solid mixture after heating is ended, adding ammonium hydroxide into the solid mixture, centrifuging, removing a precipitate, and collecting the supernatant; adding an internal standard solution into the supernatant, and uniformly mixing; and optimizing the ICP-MS to an optimal state, testing content of chlorine in the supernatant under a condition of medium resolution m/&#x394;m=4000, and testing content of bromine and iodine in the supernatant under a condition of low resolution m/&#x394;m=300.

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Hubei, China

Zhaochu Hu