Takeda Chemical Industries, Inc.

Yorifumi Ikeda

Yasuhiro Tsujimoto

Kikuo Nishikawa

Akira Nakatani

Shoichi Mori

A countercurrent liquid-solid contacting apparatus comprises a liquid purifying column for substantially purifying a liquid by passing the liquid upwardly through a bed of purifying material and a regenerating column for regenerating the purifying material used to purify the liquid. The liquid purifying column includes supply and transfer ports defined respectively at the top and bottom thereof and has therein the bed of purifying material which is spaced a predetermined distance from the top of the liquid treating column to provide a vacant space. The purifying column further includes a liquid inlet and outlet with a portion of the purifying bed above the liquid outlet serving as a settling layer to avoid any possible fluidization and/or expansion of the purifying material. The regenerating column is similar in construction to the construction of the purifying column, however, compressed air and washing liquid are successively or simultaneously supplied into the regenerating colunn to fluidize the soiled purifying material to separate suspended solids from the soiled purifying particles. The regenerated purifying material is continuously or intermittently supplied into the purifying column. A method therefor is also disclosed.

Countercurrent liquid-solid contacting apparatus

A countercurrent liquid-solid contacting apparatus having combined filtering and regenerating columns stacked one above the other. The filtering column has a liquid inlet and outlet, a liquid medium to be filtered being supplied into the filtering column through the liquid inlet and discharged to the outside through the liquid outlet after having passed upwardly through a bed of filtering material within the filtering column. The regenerating column has its bottom end opening into the filtering column and supplies a filtering material in an amount necessary to compensate for a reduction in the amount of the filtering material within the filtering column each time a portion of the filtering material in a lower region of the filtering column is withdrawn and then transported back into the regenerating column. Since the regenerating column is a closed vessel, pipe lines sealed to the atmosphere by liquid medium extending outwardly from the liquid outlet and also from the regenerating column have a predetermined relationship with each other.

A countercurrent liquid-solid contacting apparatus comprises a liquid purifying column for substantially purifying a liquid by passing the liquid upwardly through a bed of purifying material and a regenerating column for regenerating the purifying material used fo purify the liquid. The liquid purifying column includes supply and transfer ports defined respectively at the top and bottom thereof and has therein the bed of purifying material which is spaced a predetermined distance from the top of the liquid treating column to provide a vacant space. The purifying column further includes a liquid inlet and outlet with a portion of the purifying bed above the liquid outlet serving as a settling layer to avoid any possible fluidization and/or expansion of the purifying material. The regenerating column is similar in construction to the construction of the purifying column, however, compressed air and washing liquid are successively or simultaneously supplied into the regenerating column to fluidize the soiled purifying material and separate suspended solids from the soiled purifying particles. The regenerated purifying material is continuously or intermittently supplied into the purifying column. A method therefor is also disclosed.

A liquid purification apparatus which comprises a hollow cylindrical column having a liquid rectifier and collector positioned respectively adjacent the bottom and top of the column in communication with liquid inlet and outlet. A mass of adsorbent material is accommodated within the column in such an amount that a portion of the material within the column and above the liquid collector forms a settling layer to avoid any possible fluidization and/or expansion of another portion of the material situated between the liquid rectifier and collector. The column has a material inlet at the top thereof through which material is continuously supplied into the column while a portion of the material adjacent the bottom of the column is exhausted to the outside through an outlet at the bottom of the column. The uppermost surface level of the material within the column is maintained within a predetermined range.

Growing community of inventors

Suita, Japan

Yorifumi Ikeda